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how to calculate crystallinity from XRD data using OriginPro
นอกจากการดูบทความนี้แล้ว คุณยังสามารถดูข้อมูลที่เป็นประโยชน์อื่นๆ อีกมากมายที่เราให้ไว้ที่นี่: ดูเพิ่มเติม
NanoWorld,
Reference paper:
https://doi.org/10.1088/20531591/ab0aaf
In this video, I have shown a simple approach to calculating the crystallinity of material from XRD data using OriginPro software and an Excel sheet. If you need any help or have any questions, then feel free to ask in the comment section below. For more videos, please subscribe to my channel. Thank you.
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Interpretation of SAED pattern | estimation of dspacing \u0026 (khl) values
https://www.youtube.com/watch?v=XLca_Hy2GMo
How to put a scale bar on SEM \u0026 TEM images (SEM/TEM data analysis)
https://www.youtube.com/watch?v=6tmbkkp4rBg
No valid atomic position available (Rietveld refinement through X’pert Highscore)
https://www.youtube.com/watch?v=ppLoZvjgad0
Negative intensities in scan data points (Rietveld refinement through X’pert Highscore)
https://www.youtube.com/watch?v=CCNgaYp6gOw
Indexing XRD peaks with Miller indices (hkl) values using X’pert Highscore software
https://www.youtube.com/watch?v=9mL5l7yUsRY
How to plot JCPDS card with the XRD data using OriginLab software
https://www.youtube.com/watch?v=jIauR6uVDOg
XRD data analysis using X’pert Highscore software
https://www.youtube.com/watch?v=TpuL4NgCMYc
Deconvolution of photoluminescence PL spectra (PL peaks fitting)
https://www.youtube.com/watch?v=9vlNGF5jXbs
How to find peak position and FWHM of XRD data
https://www.youtube.com/watch?v=yguvwX_ia_A
How to calculate crystallites (grain) size from XRD data?
https://www.youtube.com/watch?v=m8LB4A75Ec
Estimation of grain size through modifies Scherrer equation
https://www.youtube.com/watch?v=_FTOmhsHRlE
Crystallites size and strain using WH plot method
https://youtu.be/LJ9h77fN4E
Calculation of nanoparticle size through SEM image
https://www.youtube.com/watch?v=9NLoLL4kko
How to find Miller indices of XRD peaks?
https://www.youtube.com/watch?v=GIqam7DEPY4\u0026t=139s
How to calculate dspacing from XRD data?
https://www.youtube.com/watch?v=qzSrPipUnRM
How to calculate lattice constant (a, b, c) values from the XRD data?
https://www.youtube.com/watch?v=AbpQq6NyNk
How to calculate microstrain and dislocation density from XRD data?
https://youtu.be/aWJ_m4Y0ZtE
How to calculate crystallinity from XRD data?
https://www.youtube.com/watch?v=u6LwremVt30
How to smooth XRD data?
https://www.youtube.com/watch?v=EItYvqOQe5w
Baseline correction for XRD data
https://www.youtube.com/watch?v=r1lByQP4Zmc
Cyclic Voltammetry Data Analysis
https://youtu.be/MSX6ZxoU1M4
How to find bandgap energy using the Tauc plot method?
https://www.youtube.com/watch?v=vXxNrb8rmaE
How to calculate bandgap energy using the Kubelka Munk function?
https://www.youtube.com/watch?v=Ry9Jdjeh2Q
Understanding Tauc plot, 1240 (constant) and 2.303 constant
https://www.youtube.com/watch?v=tbyJjCMkDtc
How to know a material either have direct or indirect bandgap energy?
https://www.youtube.com/watch?v=dc2EHBMlyBA
DSC Data Analysis
https://www.youtube.com/watch?v=QlD3H_s5sZ8\u0026t=1s
TGA Data Analysis
https://www.youtube.com/watch?v=J4jBy_NOqEM\u0026t=2s
How to plot the double Yaxis in a single graph?
https://www.youtube.com/watch?v=yG7WZMA37k4
Electron paramagnetic resonance (EPR) data analysis (calculation of gfactor)
https://www.youtube.com/watch?v=jENNhTwGsX0
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Crystallinity (3b2)
Rate of crystallization
Controlling crystallinity
Crystallization routes
Estimate the Crystallinity from XRD Pattern using Origin Software
The calculation of crystallinity by XRD is based on the presumption that the broad peak comes from amorphous phase, the sharp peak comes from crystal phase. So you should distinguish these two kinds peak on an XRD pattern at first. In the case of you describe, the sharp peaks become slightly broad. This causes from the small size effect of crystalline. Actually, you can take the materials with small size crystalline (less than 100nm) also as amorphous state. Here amorphous is attributed to the disorder of crystal in macro scale. Only when phase segregation in macro scale happens, that is amorphous phase segregates from crystal phase, you can use XRD data to calculate crystallinity by the broad and the sharp peaks.
% Crystallinity in XRD is calculated using the formula:
% Crystallinity = (total area of crystalline peaks) / (total area of all peaks)x 100
Note : No broad peak means 100%crytallinity
EstimatetheCrystallinity XRDPattern Nanoencryption
XRD analysis (d-spacing, crystallite size, crystallinity) from data points by using Fityk
This video illustrates Xray Diffraction analysis of materials by using the freeware software Fityk and MS Excel. Specifically, it describes how to use these tools for baseline correction, peak deconvolution, calculation of area under the peak, dspacing, FWHM and crystallite size. The purpose of creating this video is to give an idea to the undergraduate students in the domain of materials science/ polymer engineering about the practical knowledge to analyze XRD data in an effective way.
Dr. Subhendu Bhandari
Department of Plastic and Polymer Engineering
Maharashtra Institute of Technology, Aurangabad, Maharashtra, India
Crystallinity, Glass Transition Temperature \u0026 Melting Temperature
In this video, we are going to be introduce more properties and structure of polymer.
Reference:
Lamellae, spherulite and fibrillar structurehttp://www.open.edu/openlearn/sciencemathstechnology/science/chemistry/introductionpolymers/contentsection5.6.1
Chewing gumhttp://www.monitor.co.ug/Magazines/HealthLiving/Chewinggummoreharmfultoyouthananythingelseyoueat/6898463352792t9vp1k/index.html
Challenger space shuttlehttps://www.pinterest.com/explore/spaceshuttlechallenger/
Challenger oringhttp://insights.globalspec.com/article/2012/challengerdisasterheedingtheethicallessons30yearson
Question markhttps://www.pinterest.com/pin/605452743627167973
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